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Description

10.5772/intechopen.82511 88 EnzorL

Hollingworth, P

the suspension was cooled to 5 C., Trifluoro-methanesulfonic acid 2,2-difluoro-ethyl ester (1.414 mL, 6.60 mmol) was added dropwise at 5 C., then the reaction mixture was allowed to slowly warm to RT, and stirred at RT for 14 h after which there was an amber solution with a small amount of suspension