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doi: 10.1016/S0140-6736(12)60520-0 2 KorogluGKaya-SezginerEYilmaz-OralDGurS

Waters) at 50 C with methanol:water:acetic acid ratio of 42.0:58.0:0.01 (v/v/v) at a flow rate of 0.3 ml min 1 that was ramped to 80.8:19.2:0.01 (v/v/v) over 11 min and then to 98:2:0.01 (v/v/v) for 5 min