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For exact volumes by vial size, see the reconstitution table above or use the Peptide Reconstitution Calculator

This latter hypothesis has yet to be tested

To a 250 mL round bottom flask containing L27-4 (560 mg, 0.56 mmol) and 10% Pd/C (186 mg) was added ethyl acetate (20 mL) and then the reaction mixture was subjected to vacuum/N 2 cycle (3) followed by another cycle of vacuum/H 2 (3)